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Diacylglycerols (DAGs) ions, instead of triacylglycerols (TAGs) ions, were established as marker indicators for an improved classification of edible oils using ultrahigh resolution mass spectrometry (UHRMS). DAGs ions can be used not only to identify triacylglycerols (TAGs) and their embedded fatty acids (FAs), but also to distinguish positional isomers of TAGs. In this work, DAGs ions were determined in edible oils by direct infusion atmospheric pressure chemical ionization-ultrahigh resolution mass spectrometry (APCI-UHRMS), where th