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We observe that the identity of the silyloxy substituent impacts the degree of planarity of the porphyrin in the solid state as well as the redox potentials.The development of earth-abundant transition-metal-based electrocatalysts with bifunctional properties (oxygen evolution reaction (OER) and hydrogen evolution reaction (HER)) is crucial to commercial hydrogen production. In this work, layered double hydroxide (LDH)-zinc oxide (ZnO) heterostructures and oxygen vacancies are constructed synchronously by plasma magnetron sputtering of
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