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The TG and DTG characterization of PMMA and complex materials prepared by ultrasonic excitation showed that the radicals generated by ultrasonic excitation were uniformly distributed and did not generate unsaturated double bonded polymers. The electrical conductivity of the Graphene/PMMA composites prepared by ultrasonic excitation at a graphene content of 1 wt% increased to 1.13 × 10-1 S/cm, which is better than that of the Graphene/PMMA prepared by in situ polymerization. This may be attributed to the ultrasound-assisted supercritica
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