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Synthesis of the needed mono- and disaccharide-based aldehydes set the stage for DCC experiments. Evaluation of the powerful combinatorial libraries (DCLs) by UPLC-MS disclosed significant amplification of four substances into the presence of GTF180. Furthermore, we discovered that derivatives for the glucose-acceptor maltose during the C1-hydroxy team act as glucose-donors as they are cleaved by GTF180. The synthesized hits show medium to low binding affinity (KD values of 0.4-10.0 mm) based on
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