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The structures of the single crystals of compounds K2UO2(tca)4(tcaH)2 (I), K4NpO2(tca)6(tcaH)(H2O)3 (II), Rb4UO2(tca)6(tcaH)(H2O)3 (III), and Cs3UO2(tca)5(tcaH)2·H2O (IV), where tca is the trichloroacetate ion, were established by X-ray diffraction analysis. The crystals of II-IV have a framework structure, whereas in the layered crystals of I, neighboring layers are connected to each other via halogen bonds. In this regard, the crystals of I possess perfect cleavage along the (001) plane the crystals are easily cut into stacks of very
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