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The chemical and thermal stability of alkali metal naphthalenides as powerful reducing agents are examined, including the type of alkali metal ([LiNaph] and [NaNaph]), the type of solvent (THF, DME), the temperature (-30 to +50 °C), and the time of storage (0 to 12 hours). The stability and concentration of [LiNaph]/[NaNaph] are quantified via UV-Vis spectroscopy and the Lambert-Beer law. As a result, the solutions of [LiNaph] in THF at low temperature turn out to be most stable. The decomposition can be related to a reductive polymeriz
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