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In this work, several attempts were made to prepare nanoceramic zirconate (Nd₂Zr₂O7) powder for pigment applications. The single pyrochlore phase, Nd₂Zr₂O7 was successfully synthesized with the aid of flux at relatively low temperature (1000 °C) upon milling the reaction mixture made from Nd₂O₃ and ZrO₂ in a tungsten carbide vial. Several characterizations were done on the thermal analysis (TG/DTA), X-ray diffraction (XRD), High-resolution scanning electron microscope (HRSEM), energy dispersive X-ray (EDX) analysis, Fourier-transform infr
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