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© The Author(s) 2020. Published by Oxford University Press.The efficacy of sulfuryl fluoride was evaluated for control of fourth-instar pecan weevil, Curculio caryae (Horn), at 25°C for a 24-h exposure. Larvae, collected as they naturally emerged from pecans, were used to artificially infest pecan nuts. Infested nuts were fumigated with six concentration by time (CT) treatment dosages of sulfuryl fluoride (0-750 g-h/m3) within air-tight, glass containers. The sulfuryl fluoride concentration in each fumigation container was analyzed 30 mi
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