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Nickel has been widely researched in the electrooxidation of borohydride due to its low cost and abundant reserves, but its catalytic activity and stability need to be improved for practical application. In this work, a Ni and P deposited nickel foam (Ni-P@NF) catalyst electrode with a unique hierarchical structure is prepared by a simple one-step electrodeposition method. The structure, morphology, and catalytic performances of Ni-P@NF are investigated systematically. The results show that Ni-P@NF exhibits excellent catalytic activity,
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