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This work demonstrates a streamlined method to engineer a rod-like porous carbon framework (RPC) confined magnetite nanoparticles composite (Fe3O4/RPC) starting from metallic iron and gallic acid (GA) solution. First, a mild redox reaction was triggered between Fe and GA to prepare a rod-shaped metal-organic framework (MOF) ferric gallate sample (Fe-GA). Then, the Fe-GA sample was calcinated to obtain a prototypic RPC supported metal iron nanoparticle intermediate sample (Fe/RPC). Finally, the Fe3O4/RPC composite was synthesized after a
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